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Laboratory module |
related labs |
developer |
| 1 |
Separation and analysis |
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1.1 |
Isolation of maltol |
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SMCM |
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1.2 |
Separation of benzocaine & benzoic acid |
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AC |
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1.3 |
Analysis of OTC analgesics |
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AC |
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1.4 |
Thermodynamic study of esterification |
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QCC |
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1.5 |
Extraction of fat from cookies & crackers |
⇒9.5 |
AC |
| 2 |
Substitution reactions |
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2.1 |
Nucleophilic substitution of alcohols |
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SMCM |
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2.2 |
Benzylation of 4-hydroxypropiophenone |
⇒8.7 |
AC |
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2.3 |
Alkylation of theophylline |
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AC |
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2.4 |
Synthesis of phenacetin |
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QCC |
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2.5 |
Solvolysis of t-BuCl |
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QCC |
| 3 |
Elimination reactions |
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3.1 |
Dehydration of alpha-tetralol |
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AC |
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3.2 |
Dehydration of t-amyl alcohol |
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QCC |
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3.3 |
Dehydration of cyclohexanol |
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SMCM |
| 4 |
Alkene chemistry |
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4.1 |
Bromination of stilbene |
⇒5.1 |
SMCM |
| 5 |
Alkyne chemistry |
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5.1 |
Preparation of diphenylacetylene |
4.1⇒;⇒6.1 |
SMCM |
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5.2 |
Alkyne hydration |
|
AC |
| 6 |
Pericyclic reactions |
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6.1 |
Diels-Alder: cantharidin |
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AC |
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6.2 |
Diels-Alder: maleic anhydride + cyclopentadiene |
|
QCC |
| 7 |
Aromatic chemistry |
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7.1 |
Electrophilic aromatic substitution |
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SMCM |
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7.2 |
Nitration of methyl benzoate |
|
AC |
| 8 |
Carbonyl chemistry |
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Preparation of |
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8.1 |
Jones oxidation of cyclohexanol |
|
QCC |
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8.2 |
MnO2 oxidation of diphenylmethanol |
8.10⇒ |
AC |
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8.3 |
Pinacol rearrangement |
|
QCC |
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8.4 |
Synthesis of cyclohexanone (decarboxylation) |
|
QCC |
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8.5 |
Oxidative cleavage of diols |
|
SMCM |
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Reactions of |
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8.6 |
Reduction of acetophenone |
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AC |
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8.7 |
Reduction of 4-benzyloxypropiophenone |
2.2⇒ |
AC |
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8.8 |
Reduction of cyclohexanone |
|
QCC |
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8.9 |
Grignard: 2-methyl-2-hexanone |
|
QCC |
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8.10 |
Grignard: diphenylmethanol |
⇒8.2 |
AC |
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8.11 |
Aldol condensation |
|
QCC |
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8.12 |
Wittig reaction |
|
AC |
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8.13 |
Grignard: triphenylmethanol |
|
AC |
| 9 |
Carboxylic acid derivatives |
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9.1 |
Nitrile hydrolysis |
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AC |
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9.2 |
Esterification |
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SMCM |
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9.3 |
Preparation of ethyl 4-nitrobenzoate |
⇒10.1 |
AC |
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9.4 |
Amide formation |
|
SMCM |
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9.5 |
Preparation and analysis of fatty acid methyl esters (FAMEs) |
1.5⇒ |
AC |
| 10 |
Amine chemistry |
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10.1 |
Reduction of ethyl 4-nitrobenzoate |
9.3⇒ |
AC |
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10.2 |
Diazotization and coupling |
|
AC |
| 11 |
Radical chemistry |
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11.1 |
Benzylic bromination |
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AC |
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Document label syntax: |
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x.x.1 = prelab documents |
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x.x.2 = case studies |
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x.x.3 = postlab documents |
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x.x.4 = instructor materials |
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