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Technique primer |
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| P1 |
Purification |
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P1.1 |
Aqueous extraction |
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P1.2 |
Vacuum filtration |
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P1.3 |
Recrystallization |
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P1.4 |
Flash chromatography |
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P1.5 |
Distillation |
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P1.6 |
Rotary evaporation |
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| P2 |
Analysis |
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P2.1 |
Thin-layer chromatography (TLC) |
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P2.2 |
High-performance liquid chromatography (HPLC) |
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P2.3 |
Gas chromatography (GC) |
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P2.4 |
Melting point determination |
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| P3 |
Spectroscopy |
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P3.1 |
UV-Vis spectroscopy |
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P3.2 |
IR spectroscopy |
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P3.3 |
NMR spectroscopy |
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| P4 |
Calculations |
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P4.1 |
Determining yield |
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P4.2 |
Scaling reactions |
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| P5 |
General techniques |
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P5.1 |
Quantitative transfer |
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P5.2 |
Microwave-assisted synthesis (MAOS) |
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P5.3 |
Reflux |
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P5.4 |
Working under inert atmosphere |
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